How To Manufacture The D Enantiomer Of Phenylaminopropane, And 3,4,Methyl-Ene-Di

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How To Manufacture The D Enantiomer Of Phenylaminopropane, And 3,4,Methyl-Ene-Dioxymeth-Phenylaminopropane

Re: DETAILED METHODS for NON-CHEMISTS
METHamphetamine PRECURSS CLEANING/wkUP
Extractomania........by Ozbee friends..........edited by Placebo
INDEX:
1: Equipment
2: Ingredients
3: Method
step 1:
step 2:
step 3:
step 4:
step 5:
step 6:
4: Acid/Base
5: HCl-Gassing
6: Notes
1: Equipment
* Various jars, glass vessels, beakers etc
* PH paper, electronic PH tester
* Filter paper coffeee filters
* A strainer that will fit your filters nicely,
so that you get better surface area then a funnel
* Hair dryer, heat lamps
* Hot plate, no open flames, only heat elements
* Seperaty funnel, similar, tube to siphon
2: Ingredients
-Pills containing psuedo-ephedrine HCl ephedrine HCl.
-NaOH/Sodium Hydroxide/caustic soda/strong base/lye.
-Epsom salts that have been baked in oven 200c f an hour to dry.
-Methanol
-Acetone
-Toluene
-Distillated water
3: Method
***e*** :
If pills have red coating, put in jar, with acetone, shake until red coating is dissolved then continue as
below.
Step 1: First, put your pills in a jar.
Add methanol about double the volume of the pills.
Cap the jar shake till they break apart.
Leave to sit f a few hours shaking every 1/2 hour.
Let settle into 2 nice layers then siphon decant off top layer.
No need to get it all as we will do this 2 me times to be sure get all that pseudo.
step 2: Once you have done it 3 times have the 3 lots of methanol from above, put them together
put in freezer.
You want to get it real cold, near freezing then filter it thru a very fine filter, this may take some time if
you don't have a vacuum filtration setup but thats ok, we aint in a hurry.
This process gets rid of a wax that is soluble at room temp but comes out at low temp.
step 3:***e*** : This step is necessary only speeds things up.
After the chilled filter, we will reduce the volume of methanol/pseudo solution.
So, with good ventilation a fan blowing over pot, just reduce the volume of methanol, but till you
see crystals anything. Just reduce it to a manageable amount, we just want a saturated solution, you'll
ice it thicken a bit. Stop, take it off.
step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirr glass table f
fast evapation, you could just leave it laying around a couple of days let nature take its course,
it does make pretty crystals. Scrape all your crystals up when they are dry put into aher clean pyrex
v...

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